Structures by: Castillo J. C.

Total: 56

C22H25N3O2

C22H25N3O2

Galvez, JaimeCastillo, Juan-CarlosQuiroga, JairoRajzmann, MichelRodriguez, JeanCoquerel, Yoann

Organic letters (2014) 16, 16 4126-4129

a=11.1623(3)Å   b=13.0760(4)Å   c=27.158(1)Å

α=90°   β=90°   γ=90°

C29H33N3O2

C29H33N3O2

Galvez, JaimeCastillo, Juan-CarlosQuiroga, JairoRajzmann, MichelRodriguez, JeanCoquerel, Yoann

Organic letters (2014) 16, 16 4126-4129

a=25.7585(6)Å   b=10.3249(2)Å   c=9.5675(2)Å

α=90°   β=90°   γ=90°

C16H15N3

C16H15N3

Castillo, Juan-CarlosQuiroga, JairoAbonia, RodrigoRodriguez, JeanCoquerel, Yoann

Organic letters (2015) 17, 13 3374-3377

a=9.7773(2)Å   b=6.90436(13)Å   c=9.79548(19)Å

α=90.0°   β=98.985(2)°   γ=90.0°

C21H15N3

C21H15N3

Castillo, Juan-CarlosQuiroga, JairoAbonia, RodrigoRodriguez, JeanCoquerel, Yoann

Organic letters (2015) 17, 13 3374-3377

a=14.0946(2)Å   b=11.4421(2)Å   c=9.74761(17)Å

α=90.0°   β=99.2056(17)°   γ=90.0°

7-(4-Chlorophenyl)-3-iodo-2-methylpyrazolo[1,5-a]pyrimidine

C13H9ClIN3

Castillo, Juan-CarlosRosero, Hernán-AlejandroPortilla, Jaime

RSC Adv. (2017) 7, 45 28483

a=8.1315(6)Å   b=12.4851(8)Å   c=14.5014(7)Å

α=105.748(5)°   β=105.605(6)°   γ=99.832(6)°

1,3,5-tris(2-(tert-Butyl)pyrazolo[1,5-a]pyrimidin-7-yl)benzene

C150H162N36

Castillo, Juan-CarlosRosero, Hernán-AlejandroPortilla, Jaime

RSC Adv. (2017) 7, 45 28483

a=14.6829(3)Å   b=14.6829(3)Å   c=57.9972(11)Å

α=90°   β=90°   γ=120°

(5-Amino-3-methylsulfanyl-1<i>H</i>-1,2,4-triazol-1-yl)(2-fluorophenyl)methanon

C10H9FN4OS

Moreno-Fuquen, RodolfoArango-Daraviña, KevinBecerra, DianaCastillo, Juan-CarlosKennedy, Alan R.Macías, Mario A.

Acta Crystallographica Section C (2019) 75, 3

a=7.6599(9)Å   b=7.8079(8)Å   c=10.0140(12)Å

α=94.487(9)°   β=108.668(11)°   γ=97.565(9)°

2-Fluoro-<i>N</i>-(3-methylsulfanyl-1<i>H</i>-1,2,4-triazol-5-yl)benzamide

C10H9FN4OS

Moreno-Fuquen, RodolfoArango-Daraviña, KevinBecerra, DianaCastillo, Juan-CarlosKennedy, Alan R.Macías, Mario A.

Acta Crystallographica Section C (2019) 75, 3

a=5.0509(11)Å   b=26.640(5)Å   c=8.0251(16)Å

α=90°   β=94.12(2)°   γ=90°

(<i>E</i>)-1-<i>tert</i>-Butyl-5-[(2,4-dichlorobenzylidene)amino]-1<i>H</i>-pyrrole-3-carbonitrile

C16H15Cl2N3

Macías, Mario A.Castillo, Juan-CarlosPortilla, Jaime

Acta Crystallographica Section C (2018) 74, 1 82-93

a=6.5428(7)Å   b=7.9586(11)Å   c=30.415(5)Å

α=90°   β=92.987(13)°   γ=90°

(<i>E</i>)-1-<i>tert</i>-butyl-5-[(4-chlorobenzylidene)amino]-1<i>H</i>-pyrrole-3-carbonitrile

C16H16ClN3

Macías, Mario A.Castillo, Juan-CarlosPortilla, Jaime

Acta Crystallographica Section C (2018) 74, 1 82-93

a=8.8317(14)Å   b=24.261(3)Å   c=6.9706(14)Å

α=90°   β=90°   γ=90°

(<i>E</i>)-1-<i>tert</i>-Butyl-5-[(pyridin-4-ylmethylene)amino]-1<i>H</i>-pyrrole-3-carbonitrile

C15H16N4

Macías, Mario A.Castillo, Juan-CarlosPortilla, Jaime

Acta Crystallographica Section C (2018) 74, 1 82-93

a=8.1494(8)Å   b=9.0629(10)Å   c=9.4859(9)Å

α=92.465(8)°   β=97.113(8)°   γ=97.136(9)°

1-<i>tert</i>-Butyl-5-[(2,4-dichlorobenzyl)amino]-1<i>H</i>-pyrrole-3-carbonitrile

C16H17Cl2N3

Macías, Mario A.Castillo, Juan-CarlosPortilla, Jaime

Acta Crystallographica Section C (2018) 74, 1 82-93

a=8.9700(12)Å   b=9.3244(12)Å   c=10.4645(14)Å

α=105.057(12)°   β=103.589(12)°   γ=95.078(11)°

1-<i>tert</i>-Butyl-5-[(4-chlorobenzyl)amino]-1<i>H</i>-pyrrole-3-carbonitrile

C16H18ClN3

Macías, Mario A.Castillo, Juan-CarlosPortilla, Jaime

Acta Crystallographica Section C (2018) 74, 1 82-93

a=8.2422(10)Å   b=9.2361(10)Å   c=20.623(2)Å

α=90°   β=98.521(11)°   γ=90°

2-fluoro-N-(thiazol-2-yl)benzamide

C10H7FN2OS

Moreno-Fuquen, RodolfoCastillo, Juan C.Becerra, DianaCamargo, HernandoHenao, José A.

Acta Crystallographica Section E (2015) 71, 11 o882-o883

a=12.2171(8)Å   b=5.0741(3)Å   c=15.7078(10)Å

α=90.0000°   β=98.820(6)°   γ=90.000°

(+-)-3-[(Benzo[<i>d</i>][1,3]dioxol-5-yl)methyl]-2-(3,4,5-trimethoxyphenyl)-1,3-thiazolidin-4-one

C20H21NO6S

Moreno-Fuquen, RodolfoCastillo, Juan C.Abonia, RodrigoEllena, JavierDe Simone, Carlos A.

Acta Crystallographica Section E (2014) 70, 12 o1235-o1236

a=15.3098(11)Å   b=14.3677(12)Å   c=8.6546(3)Å

α=90.00°   β=97.429(4)°   γ=90.00°

3-[(<i>E</i>)-(3-<i>tert</i>-Butyl-1-phenyl-1<i>H</i>-pyrazol-5- yl)iminomethyl]quinolin-2(1<i>H</i>)-one

C23H22N4O

Castillo, Juan C.Abonía, RodrigoHursthouse, Michael B.Cobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2009) 65, 10 o495-o497

a=6.3601(2)Å   b=11.2750(5)Å   c=13.8028(5)Å

α=105.972(2)°   β=91.253(3)°   γ=98.539(2)°

5-Benzylamino-3-<i>tert</i>-butyl-1-phenyl-1<i>H</i>-pyrazole

C20H23N3

Castillo, Juan C.Abonía, RodrigoCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2009) 65, 6 o303-o310

a=20.038(4)Å   b=7.3732(12)Å   c=23.444(3)Å

α=90.00°   β=106.007(13)°   γ=90.00°

3-<i>tert</i>-butyl-5-(4-methylbenzylamino)-1-phenyl-1<i>H</i>-pyrazole

C21H25N3

Castillo, Juan C.Abonía, RodrigoCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2009) 65, 6 o303-o310

a=10.7749(13)Å   b=10.7749(13)Å   c=30.868(3)Å

α=90.00°   β=90.00°   γ=90.00°

3-<i>tert</i>-butyl-1-phenyl-5-[4-(trifluoromethyl)benzyl]-1<i>H</i>-pyrazole

C21H22F3N3

Castillo, Juan C.Abonía, RodrigoCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2009) 65, 6 o303-o310

a=20.824(3)Å   b=7.3429(11)Å   c=24.225(4)Å

α=90.00°   β=97.275(11)°   γ=90.00°

3-<i>tert</i>-butyl-5-(4-chlorobenzylamino)-1-phenyl-1<i>H</i>-pyrazole

C20H22ClN3

Castillo, Juan C.Abonía, RodrigoCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2009) 65, 6 o303-o310

a=9.385(3)Å   b=9.7584(19)Å   c=10.6014(17)Å

α=112.459(13)°   β=95.721(18)°   γ=99.735(19)°

5-(4-bromobenzyl)-3-<i>tert</i>-butyl-1-phenyl-1<i>H</i>-pyrazole

C20H22BrN3

Castillo, Juan C.Abonía, RodrigoCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2009) 65, 6 o303-o310

a=20.1981(6)Å   b=7.3960(9)Å   c=24.171(4)Å

α=90.00°   β=98.634(7)°   γ=90.00°

3-<i>tert</i>-butyl-5-(4-nitrobenzylamino)-1-phenyl-1<i>H</i>-pyrazole

C20H22N4O2

Castillo, Juan C.Abonía, RodrigoCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2009) 65, 6 o303-o310

a=9.6594(11)Å   b=12.3991(11)Å   c=15.4338(15)Å

α=90.00°   β=97.744(8)°   γ=90.00°

<i>N</i>-(3-<i>tert</i>-Butyl-1-phenyl-1<i>H</i>-pyrazol-5-yl)-<i>N</i>- (4-methoxybenzyl)acetamide

C23H27N3O2

Castillo, Juan C.Abonía, RodrigoHursthouse, Michael B.Cobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2010) 66, 2 o64-o66

a=9.8325(3)Å   b=9.8649(4)Å   c=12.0365(3)Å

α=97.468(2)°   β=95.512(2)°   γ=114.6430(10)°

4-(2-Chlorophenyl)pyrrolo[1,2-<i>a</i>]quinoxaline

C17H11ClN2

Castillo, Juan C.Abonía, RodrigoCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2013) 69, 5 544-548

a=13.5649(13)Å   b=11.8142(11)Å   c=8.1678(12)Å

α=90.00°   β=99.281(10)°   γ=90.00°

(<i>RS</i>)-4-(1,3-Benzodioxol-6-yl)-4,5-dihydropyrrolo[1,2-<i>a</i>]quinoxaline

C18H14N2O2

Castillo, Juan C.Abonía, RodrigoCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2013) 69, 5 544-548

a=26.590(3)Å   b=6.2890(9)Å   c=17.2655(19)Å

α=90.00°   β=104.017(11)°   γ=90.00°

Dibenzylammonium hydrogen maleate

C14H16N,C4H3O4

Castillo, Juan C.Abonía, RodrigoCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2013) 69, 7 798-802

a=5.7551(5)Å   b=16.1579(19)Å   c=17.1230(19)Å

α=90.00°   β=95.464(8)°   γ=90.00°

Bis(dibenzylamino)methane

C29H30N2

Castillo, Juan C.Abonía, RodrigoCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2013) 69, 7 798-802

a=25.548(6)Å   b=12.9426(16)Å   c=18.555(3)Å

α=90.00°   β=130.428(11)°   γ=90.00°

7-Benzyl-3-<i>tert</i>-butyl-1-phenyl-6,7-dihydro-1<i>H</i>,4<i>H</i>-\ pyrazolo[3,4-<i>d</i>][1,3]oxazine

C22H25N3O

Castillo, Juan C.Abonía, RodrigoCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2009) 65, 8 o423-o430

a=8.8930(10)Å   b=11.1321(12)Å   c=10.2078(9)Å

α=90.00°   β=109.749(7)°   γ=90.00°

3-<i>tert</i>-butyl-7-(4-methoxybenzyl)-1-phenyl-6,7-dihydro- 1<i>H</i>,4<i>H</i>-pyrazolo[3,4-<i>d</i>][1,3]oxazine

C23H27N3O2

Castillo, Juan C.Abonía, RodrigoCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2009) 65, 8 o423-o430

a=9.1888(2)Å   b=11.4499(3)Å   c=9.7210(2)Å

α=90.00°   β=101.8570(10)°   γ=90.00°

3-<i>tert</i>-butyl-1-phenyl-7-[4-(trifluoromethyl)benzyl]-6,7-dihydro- 1<i>H</i>,4<i>H</i>-pyrazolo[3,4-<i>d</i>][1,3]oxazine

C23H24F3N3O

Castillo, Juan C.Abonía, RodrigoCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2009) 65, 8 o423-o430

a=9.0277(11)Å   b=9.8597(12)Å   c=12.6835(18)Å

α=85.531(11)°   β=74.180(11)°   γ=67.162(9)°

3-<i>tert</i>-butyl-7-(2,3-dimethoxybenzyl)-1-phenyl-6,7-dihydro- 1<i>H</i>,4<i>H</i>-pyrazolo[3,4-<i>d</i>][1,3]oxazine

C24H29N3O3

Castillo, Juan C.Abonía, RodrigoCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2009) 65, 8 o423-o430

a=8.8268(10)Å   b=11.6521(10)Å   c=10.3831(7)Å

α=90.00°   β=93.747(9)°   γ=90.00°

3-<i>tert</i>-butyl-1-phenyl-7-(3,4,5-trimethoxybenzyl)-6,7-dihydro- 1<i>H</i>,4<i>H</i>-pyrazolo[3,4-<i>d</i>][1,3]oxazine

C25H31N3O4

Castillo, Juan C.Abonía, RodrigoCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2009) 65, 8 o423-o430

a=9.8189(10)Å   b=10.0499(8)Å   c=12.8130(14)Å

α=68.710(9)°   β=72.537(8)°   γ=70.982(8)°

3-<i>tert</i>-butyl-7-(3,4-methylenedioxybenzyl)-1-phenyl-6,7-dihydro- 1<i>H</i>,4<i>H</i>-pyrazolo[3,4-<i>d</i>][1,3]oxazine

C23H25N3O3

Castillo, Juan C.Abonía, RodrigoCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2009) 65, 8 o423-o430

a=9.1164(14)Å   b=11.3303(18)Å   c=19.694(2)Å

α=90.00°   β=99.775(13)°   γ=90.00°

3-<i>tert</i>-butyl-7-(4-nitrobenzyl)-1-phenyl-6,7-dihydro- 1<i>H</i>,4<i>H</i>-pyrazolo[3,4-<i>d</i>][1,3]oxazine

C22H24N4O3

Castillo, Juan C.Abonía, RodrigoCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2009) 65, 8 o423-o430

a=19.164(2)Å   b=8.7781(7)Å   c=11.7188(12)Å

α=90.00°   β=101.717(10)°   γ=90.00°

2-methoxy-4-(pyrrolo[1,2-<i>a</i>]quinoxalin-4-yl)phenol

C18H14N2O2

Castillo, Juan C.Abonía, RodrigoCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2010) 66, 8 o385-o388

a=7.9278(8)Å   b=15.2929(18)Å   c=22.410(4)Å

α=90.00°   β=90.326(12)°   γ=90.00°

2-methoxy-4-(pyrrolo[1,2-<i>a</i>]quinoxalin-4-yl)phenol

C18H14N2O2

Castillo, Juan C.Abonía, RodrigoCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2010) 66, 8 o385-o388

a=7.9278(8)Å   b=15.2929(18)Å   c=22.410(4)Å

α=90.00°   β=90.326(12)°   γ=90.00°

3-Diphenylaminoisobenzofuran-1(3H)-one

C20H15NO2

Moreno-Fuquen, RodolfoCastillo, Juan C.Abonia, RodrigoEllena, JavierTenorio, Juan C.

Acta Crystallographica Section E (2014) 70, 4 o490

a=19.1440(13)Å   b=8.9363(6)Å   c=9.1111(3)Å

α=90.00°   β=90.00°   γ=90.00°

(+-)-3-(5-Amino-3-methyl-1-phenyl-1<i>H</i>-pyrazol-4-yl)-2-benzofuran-1(3<i>H</i>)-one

C18H15N3O2

Moreno-Fuquen, RodolfoCastillo, Juan C.Abonia, RodrigoEllena, JavierTenorio, Juan C.

Acta Crystallographica Section E (2013) 69, 7 o1181-o1182

a=10.0451(2)Å   b=15.0631(5)Å   c=12.2008(4)Å

α=90.00°   β=123.257(2)°   γ=90.00°

C72H60Cu4I4P4[solvent]

C72H60Cu4I4P4[solvent]

Castillo, Juan-CarlosBravo, Nestor-FabianTamayo, Lenka-VictoriaMestizo, Paula-DanielaHurtado, JohnMacías, MarioPortilla, Jaime

ACS omega (2020) 5, 46 30148-30159

a=18.3661(16)Å   b=16.0719(14)Å   c=27.117(3)Å

α=90°   β=108.602(10)°   γ=90°

C29H31CuIN4P

C29H31CuIN4P

Castillo, Juan-CarlosBravo, Nestor-FabianTamayo, Lenka-VictoriaMestizo, Paula-DanielaHurtado, JohnMacías, MarioPortilla, Jaime

ACS omega (2020) 5, 46 30148-30159

a=10.7747(8)Å   b=15.4475(10)Å   c=19.6421(12)Å

α=109.743(6)°   β=99.759(5)°   γ=103.575(6)°

C14H11N3O

C14H11N3O

Castillo, Juan-CarlosTigreros, AlexisPortilla, Jaime

The Journal of organic chemistry (2018) 83, 18 10887-10897

a=14.466(2)Å   b=7.8330(15)Å   c=20.727(4)Å

α=90°   β=98.549(15)°   γ=90°

C12H12O4

C12H12O4

Castillo, Juan-CarlosCastro-Agudelo, BrianGálvez, JaimeCarissan, YannickRodríguez, JeanCoquerel, Yoann

The Journal of organic chemistry (2020)

a=6.7935(2)Å   b=8.8102(3)Å   c=9.8737(4)Å

α=101.487(2)°   β=108.498(2)°   γ=106.224(2)°

4(C8H10O3),H2O

4(C8H10O3),H2O

Castillo, Juan-CarlosCastro-Agudelo, BrianGálvez, JaimeCarissan, YannickRodríguez, JeanCoquerel, Yoann

The Journal of organic chemistry (2020)

a=9.7851(2)Å   b=10.0054(3)Å   c=17.1038(4)Å

α=99.977(2)°   β=101.184(2)°   γ=90.391(2)°

C23H21N3O4

C23H21N3O4

Charris-Molina, AndrésCastillo, Juan-CarlosMacías, MarioPortilla, Jaime

The Journal of organic chemistry (2017) 82, 23 12674-12681

a=10.0379(13)Å   b=10.2812(13)Å   c=10.6299(13)Å

α=73.378(11)°   β=83.687(10)°   γ=80.048(11)°

C26H25ClN4O4

C26H25ClN4O4

Charris-Molina, AndrésCastillo, Juan-CarlosMacías, MarioPortilla, Jaime

The Journal of organic chemistry (2017) 82, 23 12674-12681

a=7.0920(15)Å   b=34.990(8)Å   c=9.922(3)Å

α=90°   β=98.12(3)°   γ=90°

C26H25N4O4

C26H25N4O4

Charris-Molina, AndrésCastillo, Juan-CarlosMacías, MarioPortilla, Jaime

The Journal of organic chemistry (2017) 82, 23 12674-12681

a=7.1294(7)Å   b=32.835(3)Å   c=10.2161(9)Å

α=90°   β=96.947(9)°   γ=90°

C23H18ClN3O3

C23H18ClN3O3

Charris-Molina, AndrésCastillo, Juan-CarlosMacías, MarioPortilla, Jaime

The Journal of organic chemistry (2017) 82, 23 12674-12681

a=16.130(2)Å   b=17.057(3)Å   c=15.338(2)Å

α=90°   β=106.066(14)°   γ=90°

C28H20FN3O3,C3H7NO

C28H20FN3O3,C3H7NO

Charris-Molina, AndrésCastillo, Juan-CarlosMacías, MarioPortilla, Jaime

The Journal of organic chemistry (2017) 82, 23 12674-12681

a=10.8530(15)Å   b=12.0931(16)Å   c=12.7462(12)Å

α=111.386(10)°   β=93.203(10)°   γ=111.842(13)°

C35H31N3O

C35H31N3O

Castillo, Juan-CarlosQuiroga, JairoAbonia, RodrigoRodriguez, JeanCoquerel, Yoann

The Journal of organic chemistry (2015) 80, 19 9767-9773

a=10.1193(13)Å   b=29.068(2)Å   c=10.5161(10)Å

α=90.0°   β=111.963(13)°   γ=90.0°

C32H28ClN3

C32H28ClN3

Castillo, Juan-CarlosQuiroga, JairoAbonia, RodrigoRodriguez, JeanCoquerel, Yoann

The Journal of organic chemistry (2015) 80, 19 9767-9773

a=9.7402(4)Å   b=11.0764(5)Å   c=23.9164(11)Å

α=90.0°   β=90.0°   γ=90.0°

C10H9N3O

C10H9N3O

Castillo, Juan-CarlosEstupiñan, DiegoNogueras, ManuelCobo, JustoPortilla, Jaime

The Journal of organic chemistry (2016) 81, 24 12364-12373

a=6.8354(5)Å   b=11.3494(10)Å   c=12.1390(9)Å

α=90°   β=104.352(2)°   γ=90°

C37H34N6O7

C36H34N6O6,CO

Hemraj JuwarkerJeremy M. LenhardtJosé C. CastilloEmily ZhaoSibi KrishnamurthyRyan M. JamiolkowskiKi-Hyon KimStephen L. Craig

Journal of Organic Chemistry (2009) 74, 8924-8934

a=10.3554(19)Å   b=32.575(5)Å   c=10.4974(18)Å

α=90.00°   β=100.230(10)°   γ=90.00°

3-<i>tert</i>-butyl-5-(3,4,5-trimethoxybenzylamino)-1-phenyl-1<i>H</i>-pyrazole

C23H29N3O3

Castillo, Juan C.Abonía, RodrigoCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2009) 65, 6 o303-o310

a=10.1533(11)Å   b=11.1645(10)Å   c=20.927(2)Å

α=84.820(8)°   β=82.988(8)°   γ=63.153(7)°

3-<i>tert</i>-butyl-7-(4-methylbenzyl)-1-phenyl-6,7-dihydro- 1<i>H</i>,4<i>H</i>-pyrazolo[3,4-<i>d</i>][1,3]oxazine

C23H27N3O

Castillo, Juan C.Abonía, RodrigoCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2009) 65, 8 o423-o430

a=8.9500(7)Å   b=11.2146(10)Å   c=10.0768(9)Å

α=90.00°   β=107.572(5)°   γ=90.00°

C35H35N3O3

C35H35N3O3

Castillo, Juan-CarlosQuiroga, JairoAbonia, RodrigoRodriguez, JeanCoquerel, Yoann

The Journal of organic chemistry (2015) 80, 19 9767-9773

a=10.63570(16)Å   b=10.82044(18)Å   c=26.4828(5)Å

α=90.0°   β=91.8720(15)°   γ=90.0°